ChemicalBook CAS DataBase List 2-AMINO-1-(3-BROMO-PHENYL)-ETHANONE HYDROCHLORIDE

2-AMINO-1-(3-BROMO-PHENYL)-ETHANONE HYDROCHLORIDE synthesis

3synthesis methods

Product Name:2-AMINO-1-(3-BROMO-PHENYL)-ETHANONE HYDROCHLORIDE
CAS Number:61858-39-7
Molecular formula:C8H9BrClNO
Molecular Weight:250.52

18523-22-3 Synthesis

18523-22-3
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2-AMINO-1-(3-BROMO-PHENYL)-ETHANONE HYDROCHLORIDE

61858-39-7
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Yield:-

Reaction Conditions:

with concentrated aqueous hydrochloric acid;hexamethylenetetramine in ethanol;dichloromethane

Steps:

4 Example 4
A solution of m-bromophenacyl bromide (38.9 g.) in methylene chloride (50 ml.) was added to a stirred solution of hexamethylenetetramine (20.1 g.) in methylene chloride (230 ml.) and the mixture was stirred at laboratory temperature for 2 hours and then filtered. The solid residue (after washing with methylene chloride and drying) was added to a stirred mixture of ethanol (100 ml.) and concentrated aqueous hydrochloric acid (45 ml.) and the mixture was stirred at laboratory temperature for 17 hours and filtered. The solid product was washed with ethanol, and there was thus obtained 2-m-bromophenyl-2-oxoethylamine hydrochloride.

References:

Imperial Chemical Industries, PLC US4489074, 1984, A

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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61858-39-7
58 suppliers
$78.00/250mg

References

1000210-73-0
0 suppliers
inquiry

61858-39-7
58 suppliers
$78.00/250mg

References