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2-Amino-1-bromonaphthalene synthesis
- Product Name:2-Amino-1-bromonaphthalene
- CAS Number:20191-75-7
- Molecular formula:C10H8BrN
- Molecular Weight:222.08
![2-AMINO-1-BROMONAPHTHALENE 2-AMINO-1-BROMONAPHTHALENE](/NewsImg/2024-04-08/6384817950788511157498867.png)
![2-Naphthoic acid](/CAS/GIF/93-09-4.gif)
93-09-4
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20191-75-7
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: diphenyl phosphoryl azide; triethylamine / toluene / 24 h / Molecular sieve; Heating / reflux
2: hydrogenchloride / ethyl acetate / 1 h
3: N-Bromosuccinimide; toluene-4-sulfonic acid / tetrahydrofuran / 5 h / 0 - 23 °C
References:
THE SCRIPPS RESEARCH INSTITUTE WO2009/64908, 2009, A1
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20191-75-7
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