2-AMINO-3-CHLOROBENZAMIDE synthesis

5synthesis methods

Product Name:2-AMINO-3-CHLOROBENZAMIDE
CAS Number:18343-44-7
Molecular formula:C7H7ClN2O
Molecular Weight:170.6

6388-47-2 Synthesis

6388-47-2
291 suppliers
$8.00/5g

18343-44-7
23 suppliers
$62.50/250mg

Yield:18343-44-7 97%

Reaction Conditions:

Stage #1: 2-amino-3-chlorobenzoic acidwith 1,1'-carbonyldiimidazole in N,N-dimethyl-formamide at 70; for 1 h;Inert atmosphere;
Stage #2: with ammonium hydroxide in N,N-dimethyl-formamide;

References:

Nathubhai, Amit;Patterson, Richard;Woodman, Timothy J.;Sharp, Harriet E. C.;Chui, Miranda T. Y.;Chung, Hugo H. K.;Lau, Stephanie W. S.;Zheng, Jun;Lloyd, Matthew D.;Thompson, Andrew S.;Threadgill, Michael D. [Organic and Biomolecular Chemistry,2011,vol. 9,# 17,p. 6089 - 6099] Location in patent:experimental part

7477-63-6 Synthesis