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2-AMino-4-chlorothiobenzaMide, 97% synthesis

1synthesis methods
-

Yield:2586-93-8 78%

Reaction Conditions:

with sodium hydrogen sulfide monohydrate;magnesium chloride in N,N-dimethyl-formamide at 20; for 72 h;Sealed tube;

References:

Oschatz, Stefan;Brunzel, Tom;Wu, Xiao-Feng;Langer, Peter [Organic and Biomolecular Chemistry,2015,vol. 13,# 4,p. 1150 - 1158]