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2-Amino-5-ethylthiophene synthesis

2synthesis methods
-

Yield:63806-77-9 37%

Reaction Conditions:

with O-(4-nitrobenzoyl)hydroxylammonium trifluoromethanesulfonate;iron(II) bromide;silver(I) triflimide in 2,2,2-trifluoroethanol;water at 30; for 2 h;

References:

Liu, Jianzhong;Wu, Kai;Shen, Tao;Liang, Yujie;Zou, Miancheng;Zhu, Yuchao;Li, Xinwei;Li, Xinyao;Jiao, Ning [Chemistry - A European Journal,2017,vol. 23,# 3,p. 563 - 567] Location in patent:supporting information