ChemicalBook CAS DataBase List 2-Amino-6-chlorobenzaldehyde

2-Amino-6-chlorobenzaldehyde synthesis

5synthesis methods

Product Name:2-Amino-6-chlorobenzaldehyde
CAS Number:35490-90-5
Molecular formula:C7H6ClNO
Molecular Weight:155.58

39885-08-0 Synthesis

39885-08-0
81 suppliers
$6.00/100mg

35490-90-5
56 suppliers
$21.00/100mg

Yield:35490-90-5 96%

Reaction Conditions:

with manganese(IV) oxide in diethyl ether; for 0.5 h;

Steps:

10

To prepare this compound, manganese dioxide (13.6 g, 157 mmol) was added to a solution of 2-(amino-6-chlorophenyl)methanol (2.75 g, 17.5 mmol) in 150 mL diethyl ether. The mixture was stirred for 0.5 hours then filtered through celite and rinsed with ethyl acetate. The filtrate was concentrated under reduced pressure to afford 2.62 g(96%) of 2-amino-6-chlorobenzaldehyde.

References:

WO2006/10142,2006,A2 Location in patent:Page/Page column 70; 71

6361-22-4 Synthesis