2-Amino-p-cresol synthesis
- Product Name:2-Amino-p-cresol
- CAS Number:95-84-1
- Molecular formula:C7H9NO
- Molecular Weight:123.15
119-33-5
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95-84-1
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Yield:95-84-1 100%
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in methanol at 23; for 5 h;
Steps:
81
To a solution of 4-methyl-2-nitrophenol (1.0 g, 6.53 mmol) in methanol (10 mL) at 23° C. was added Pd/C (10 wt %, 400 mg), and the reaction mixture was deoxygenated under vacuum, then purged with hydrogen in a balloon. After stirring for 5 h, the reaction mixture was filtered through a pad of Celite and the Celite pad was rinsed with methanol (100 mL). The filtrate was concentrated in vacuo to yield 2-amino-4-methylphenol (803 mg, 100%).
References:
VICURON PHARMACEUTICALS INC. US2006/211603, 2006, A1 Location in patent:Page/Page column 68
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95-54-5
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95-84-1
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2440-22-4
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95-54-5
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$9.00/1g
95-84-1
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$6.00/10g
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952-47-6
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95-84-1
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