2-aminopropan-1-ol hydrochloride synthesis
- Product Name:2-aminopropan-1-ol hydrochloride
- CAS Number:6170-23-6
- Molecular formula:C3H10ClNO
- Molecular Weight:111.5706
99418-53-8
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Yield:6170-23-6 74%
Reaction Conditions:
Stage #1: 2,2,2-trichloro-acetimidic acid propyl esterwith N-iodo-succinimide in 1,2-dichloro-ethane at 110; for 3 h;Inert atmosphere;Sealed tube;
Stage #2: with hydrogenchloride in tetrahydrofuran;water;1,2-dichloro-ethane at 20; for 5 h;Inert atmosphere;Sealed tube;
References:
Mou, Xue-Qing;Chen, Xiang-Yu;Chen, Gong;He, Gang [Chemical Communications,2018,vol. 54,# 5,p. 515 - 518] Location in patent:supporting information
116-09-6
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$11.00/25g
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