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2-(Anthracen-9-yl)-2H-pyran-4(3H)-one synthesis

1synthesis methods
54125-02-9 Synthesis
1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE

54125-02-9
99 suppliers
$48.61/1g

2-(Anthracen-9-yl)-2H-pyran-4(3H)-one

1315503-47-9
4 suppliers
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Yield:1315503-47-9 53%

Reaction Conditions:

with boron trifluoride diethyl etherate in dichloromethane at -78; for 8 h;Inert atmosphere;Diels-Alder reaction;

References:

Jaber, Deana M.;Burgin, Ryan N.;Hepler, Matthew;Zavalij, Peter;Doyle, Michael P. [Chemical Communications,2011,vol. 47,# 27,p. 7623 - 7625] Location in patent:supporting information; experimental part