2-AZEPAN-1-YL-BENZYLAMINE synthesis
1synthesis methods
- Product Name:2-AZEPAN-1-YL-BENZYLAMINE
- CAS Number:72752-55-7
- Molecular formula:C13H20N2
- Molecular Weight:204.31
Yield:72752-55-7 75%
Reaction Conditions:
Stage #1: hexamethylene iminewith dimethylsulfide borane complex in tetrahydrofuran at 0;
Stage #2: with n-butyllithium in tetrahydrofuran;hexane at 0;
Stage #3: 2-fluorobenzonitrile in tetrahydrofuran;hexane at 65; for 2 h;Further stages.;
References:
Thomas;Collins;Cuzens;Spiciarich;Goralski;Singaram [Journal of Organic Chemistry,2001,vol. 66,# 6,p. 1999 - 2004]