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ChemicalBook CAS DataBase List 2'-AZIDO-D-ADENOSINE

2'-AZIDO-D-ADENOSINE synthesis

11synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 77 percent / triethylamine, DMAP / CH2Cl2 / 0.5 h / Ambient temperature
2: 90 percent / LiCl / hexamethylphosphoric acid triamide / 1 h / Ambient temperature
3: 84 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.17 h / Ambient temperature

References:

Fukukawa;Uedao;Hirano [Chemical and Pharmaceutical Bulletin,1983,vol. 31,# 5,p. 1582 - 1592]

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