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2-Azidobiphenyl synthesis

11synthesis methods
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Yield:7599-23-7 100%

Reaction Conditions:

Stage #1: 2-phenylanilinewith acetic acid;sodium nitrite in water at 0; for 1 h;Cooling with ice;Inert atmosphere;
Stage #2: with sodium azide in water at 0 - 20;Inert atmosphere;

References:

Stokes, Benjamin J.;Jovanovic, Brankica;Dong, Huijun;Richert, Kathleen J.;Riell, Ryan D.;Driver, Tom G. [Journal of Organic Chemistry,2009,vol. 74,# 8,p. 3225 - 3228] Location in patent:supporting information; experimental part