2-((Benzyloxy)methyl)-4-methoxy-1-vinylbenzene synthesis

4synthesis methods

Product Name:2-((Benzyloxy)methyl)-4-methoxy-1-vinylbenzene
CAS Number:842167-45-7
Molecular formula:C17H18O2
Molecular Weight:254.32

150192-39-5
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2-((Benzyloxy)methyl)-4-methoxy-1-vinylbenzene

842167-45-7
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 100 percent / NaH / tetrahydrofuran / 0 - 20 °C
2: 91 percent / n-BuLi / tetrahydrofuran; hexane / -78 - 20 °C
3: 98 percent / n-BuLi / tetrahydrofuran; hexane / 4.5 h / 20 °C

References:

Ikeuchi, Yutaka;Taguchi, Takeo;Hanzawa, Yuji [Journal of Organic Chemistry,2005,vol. 70,# 2,p. 756 - 759]

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842167-45-7
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References

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References

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References