2-BroMo-3-iodo-1,4-diMethoxybenzene, 97% synthesis
- Product Name:2-BroMo-3-iodo-1,4-diMethoxybenzene, 97%
- CAS Number:107135-55-7
- Molecular formula:C8H8BrIO2
- Molecular Weight:342.96
25245-34-5
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107135-55-7
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Yield:107135-55-7 80%
Reaction Conditions:
Stage #1: 1-bromo-2,5-dimethoxybenzenewith lithium di-tert-butyl(2,2,6,6-tetramethylpiperidino)zincate in tetrahydrofuran at -78 - -30;
Stage #2: with iodine in tetrahydrofuran at -30 - 20;
References:
Guilarte, Veronica;Castroviejo, M. Pilar;Alvarez, Estela;Sanz, Roberto [Beilstein Journal of Organic Chemistry,2011,vol. 7,art. no. 146,p. 1255 - 1260] Location in patent:supporting information; experimental part
26002-57-3
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107135-55-7
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107135-53-5
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107135-55-7
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107135-54-6
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107135-55-7
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