ChemicalBook CAS DataBase List 2-BROMO-3-IODOPHENYL N,N-DIETHYLCARBAMATE

2-BROMO-3-IODOPHENYL N,N-DIETHYLCARBAMATE synthesis

4synthesis methods

Product Name:2-BROMO-3-IODOPHENYL N,N-DIETHYLCARBAMATE
CAS Number:863870-83-1
Molecular formula:C11H13BrINO2
Molecular Weight:398.03

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2-BROMO-3-IODOPHENYL N,N-DIETHYLCARBAMATE

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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: NaH / tetrahydrofuran / 20 °C
1.2: 95 percent / tetrahydrofuran / 8 h / 20 °C
2.1: LDA / tetrahydrofuran; hexane / 0.5 h / -78 °C
2.2: 60 percent / 1,2-dibromoethane / tetrahydrofuran; hexane / -78 - 20 °C

References:

Sanz, Roberto;Castroviejo, M. Pilar;Fernandez, Yolanda;Fananas, Francisco J. [Journal of Organic Chemistry,2005,vol. 70,# 16,p. 6548 - 6551]

Carbamic acid, N,N-diethyl-, 3-iodophenyl ester

863870-73-9
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863870-83-1
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References

88-10-8 Synthesis

88-10-8
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863870-83-1
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References

626-02-8
287 suppliers
$9.00/5g

88-10-8 Synthesis

88-10-8
228 suppliers
$10.00/5g

863870-83-1
9 suppliers
inquiry

References