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2-BROMO-3-METHYL-2-CYCLOPENTEN-1-ONE synthesis

3synthesis methods
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Yield:80963-36-6 96%

Reaction Conditions:

Stage #1: 3-Methyl-2-cyclopenten-1-onewith 3,3-dimethyldioxirane in acetone at 20; for 8 h;Epoxidation;
Stage #2: with Amberlyst 15;sodium bromide in acetone at 20; for 12 h;Bromination;

References:

Righi, Giuliana;Bovicelli, Paolo;Sperandio, Anna [Tetrahedron Letters,1999,vol. 40,# 32,p. 5889 - 5892]

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