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ChemicalBook CAS DataBase List 2-Bromo-N-(2-bromophenyl)acetamide

2-Bromo-N-(2-bromophenyl)acetamide synthesis

2synthesis methods
A washed round bottom flask was taken and 10 ml of  10 % sodium carbonate solution was poured.0.1 ml of  2-bromo aniline was dispersed into the flask and was  shaken properly. Then 1 ml of acid titled acid was  added and shaken it vigorously until ppts appeared.Reaction mixture was filtered to separate the  precipitates formed. Precipitates were dried and solid product obtained was calculated.
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Yield:88369-50-0 70%

Reaction Conditions:

with pyridine in 1,4-dioxane; for 3 h;Ambient temperature;

References:

Viti, Giovanni;Giannotti, Danilo;Nannicini, Rossano;Ricci, Renzo;Pestillini, Vittorio [Journal of Heterocyclic Chemistry,1990,vol. 27,# 5,p. 1369 - 1375]