ChemicalBook CAS DataBase List 2'-Bromobiphenyl-2-amine

2'-Bromobiphenyl-2-amine synthesis

11synthesis methods

Product Name:2'-Bromobiphenyl-2-amine
CAS Number:54147-91-0
Molecular formula:C12H10BrN
Molecular Weight:248.12

615-43-0
412 suppliers
$5.00/5g

244205-40-1 Synthesis

244205-40-1
321 suppliers
$9.00/1g

54147-91-0
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Yield:54147-91-0 90%

Reaction Conditions:

Stage #1: 2-iodophenylamine;(2-bromophenyl)boronic acidwith tetrakis(triphenylphosphine) palladium⁽⁰⁾;sodium hydrogencarbonate in 1,2-dimethoxyethane at 20 - 27; under 720 - 770 Torr; for 0.0833333 h;Suzuki coupling;
Stage #2: in 1,2-dimethoxyethane;water at 120; for 3 h;

References:

Pan, Xiaohong;Wilcox, Craig S. [Journal of Organic Chemistry,2010,vol. 75,# 19,p. 6445 - 6451] Location in patent:experimental part

615-43-0
412 suppliers
$5.00/5g

244205-40-1 Synthesis

244205-40-1
321 suppliers
$9.00/1g

54147-91-0
15 suppliers
inquiry

86-74-8 Synthesis