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2-(bromomethyl)-2-ethenyl-1,3-dioxolane synthesis

1synthesis methods
1,3-Dioxolane, 2-(1-bromoethyl)-2-(bromomethyl)-

20599-03-5
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2-(bromomethyl)-2-ethenyl-1,3-dioxolane

250338-50-2
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Yield:250338-50-2 94%

Reaction Conditions:

with potassium tert-butylate in tetrahydrofuran;Steam distillation;

References:

Carlson, Rolf;Descomps, Alexandre;Mekonnen, Alemayehu;Westerlund, Andreas;Havelkova, Martina [Synthetic Communications,2011,vol. 41,# 19,p. 2939 - 2945] Location in patent:experimental part