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123528-99-4

2-Butanone, 3,3-dimethyl-4-(methylamino)- (9CI) synthesis

2synthesis methods
Methanamine, N-(3-chloro-1,2,2-trimethylpropylidene)-, (E)- (9CI)

106367-30-0
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2-Butanone, 3,3-dimethyl-4-(methylamino)- (9CI)

123528-99-4
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Yield:123528-99-4 92%

Reaction Conditions:

with sodium methylate in methanol; for 5 h;Heating;

References:

Sulmon, Paul;Kimpe, Norbert De;Schamp, Niceas [Tetrahedron,1989,vol. 45,# 10,p. 2937 - 2956]