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51432-00-9

2-CARBOETHOXY-2'-METHOXYBENZOPHENONE synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: copper(I) thiophene-2-carboxylate; rhodium (II) octanoate dimer / toluene / 6 h / 20 °C / Inert atmosphere
1.2: 8 h / 80 °C / Inert atmosphere
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 2 h / 80 °C / Inert atmosphere

References:

Luo, Han;Li, You;Du, Luan;Xin, Xiaolan;Wang, Tao;Han, Jingpeng;Tian, Yi;Li, Baosheng [Organic Letters,2021,vol. 23,# 20,p. 7883 - 7887]

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