2-CHLORO-4,6-DIMETHYL-QUINOLINE synthesis
- Product Name:2-CHLORO-4,6-DIMETHYL-QUINOLINE
- CAS Number:3913-18-6
- Molecular formula:C11H10ClN
- Molecular Weight:191.66
23947-37-7
22 suppliers
$106.00/250mg
3913-18-6
19 suppliers
$60.00/100mg
Yield:3913-18-6 70%
Reaction Conditions:
with trichlorophosphate at 80; for 3 h;
Steps:
1.3.1 1.3.1 Synthesis of Intermediate 4a
To a dry three-necked flask was added compound 3a (2 g, 11.5 mmol)And phosphorus oxychloride(16 mL, 173.2 mmol)80 reflux 3h,Cooled to room temperature, the reaction solution poured into ice water, add sodium hydroxide solution adjusted PH = 7, filtered white solid (Yield = 70%).
References:
CN107098901,2017,A Location in patent:Paragraph 0061; 0062
2415-85-2
172 suppliers
$14.00/25g
3913-18-6
19 suppliers
$60.00/100mg
23947-37-7
22 suppliers
$106.00/250mg
3913-18-6
19 suppliers
$60.00/100mg
106-49-0
388 suppliers
$5.00/5G
3913-18-6
19 suppliers
$60.00/100mg