2-Chloro-4-cyano-3-iodopyridine synthesis
- Product Name:2-Chloro-4-cyano-3-iodopyridine
- CAS Number:908279-56-1
- Molecular formula:C6H2ClIN2
- Molecular Weight:264.45
33252-30-1
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Yield:908279-56-1 68%
Reaction Conditions:
Stage #1: 2-chloro-4-pyridinenitrilewith lithium diisopropyl amide in tetrahydrofuran at -95; for 0.0333333 h;
Stage #2: with iodine in tetrahydrofuran at -95;
References:
Chang, Ching-Yao;Liu, Hui-Ming;Chow, Tahsin J. [Journal of Organic Chemistry,2006,vol. 71,# 16,p. 6302 - 6304]