ChemicalBook CAS DataBase List 2-chloro-6-(triMethylsilyl)pyridine

2-chloro-6-(triMethylsilyl)pyridine synthesis

4synthesis methods

Product Name:2-chloro-6-(triMethylsilyl)pyridine
CAS Number:263698-97-1
Molecular formula:C8H12ClNSi
Molecular Weight:185.73

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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: BuLi; 2-(dimethylamino)ethanol / hexane / 1 h / -78 °C
1.2: 65 percent / DCl; D₂O / hexane / 0.25 h / -78 °C
2.1: 2-(dimethylamino)ethanol; BuLi / hexane / 1 h / -78 °C
2.2: 98 percent / hexane; tetrahydrofuran / 1 h / -78 - 20 °C

References:

Gros, Philippe;Choppin, Sabine;Mathieu, Julien;Fort, Yves [Journal of Organic Chemistry,2002,vol. 67,# 1,p. 234 - 237]

109-09-1
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$10.60/1gm: