![](/CAS/GIF/2142-68-9.gif)
2'-Chloroacetophenone synthesis
- Product Name:2'-Chloroacetophenone
- CAS Number:2142-68-9
- Molecular formula:C8H7ClO
- Molecular Weight:154.59
![2-Bromo-2'-chloroacetophenone](/CAS/GIF/5000-66-8.gif)
5000-66-8
245 suppliers
$14.00/1g
![2'-Chloroacetophenone](/CAS/GIF/2142-68-9.gif)
2142-68-9
386 suppliers
$6.00/10g
Yield:2142-68-9 97%
Reaction Conditions:
with diethyl ether in lithium hydroxide monohydrate at 20; for 1.5 h;Schlenk technique;Irradiation;
Steps:
3. General procedure for the reaction of reductive dehalogenation
General procedure: To a 10 mL schlenk tube, 1 (0.2 mmol), H2O (1.6 mmol) and Et2O (4 mL) were added in sequence. The reaction mixture was stirred and irradiated by 40 W Kessil purple LED (390 nm) at room temperature . After the reaction was completed, the reaction mixture was purified by flash column chromatography using PE/EtOAc as the eluent to give the desired product.
References:
Zhang, Jinrong;Chen, Jiajia;Chen, Jianhui;Luo, Yanshu;Xia, Yuanzhi [Tetrahedron Letters,2022,vol. 98,art. no. 153835] Location in patent:supporting information
![1-CHLORO-2-ETHYNYLBENZENE](/CAS/GIF/873-31-4.gif)
873-31-4
175 suppliers
$14.00/1g
![2'-Chloroacetophenone](/CAS/GIF/2142-68-9.gif)
2142-68-9
386 suppliers
$6.00/10g
![1-CHLORO-2-ETHYLBENZENE](/CAS/GIF/89-96-3.gif)
89-96-3
40 suppliers
$25.00/1g
![2'-Chloroacetophenone](/CAS/GIF/2142-68-9.gif)
2142-68-9
386 suppliers
$6.00/10g
![2-Chlorostyrene](/CAS/GIF/2039-87-4.gif)
2039-87-4
157 suppliers
$7.00/1g
![2'-Chloroacetophenone](/CAS/GIF/2142-68-9.gif)
2142-68-9
386 suppliers
$6.00/10g
![Benzene, 1-chloro-2-(1-methylethenyl)-](/CAS/20210111/GIF/3609-45-8.gif)
3609-45-8
0 suppliers
inquiry
![2'-Chloroacetophenone](/CAS/GIF/2142-68-9.gif)
2142-68-9
386 suppliers
$6.00/10g