2-CHLOROETHYLDIPHENYLPHOSPHINE synthesis
2synthesis methods
- Product Name:2-CHLOROETHYLDIPHENYLPHOSPHINE
- CAS Number:5055-11-8
- Molecular formula:C14H14ClP
- Molecular Weight:248.69
Yield:5055-11-8 78%
Reaction Conditions:
Stage #1: chloro-diphenylphosphinewith sodium in tetrahydrofuran at 90; for 28 h;Inert atmosphere;
Stage #2: 1,2-dichloro-ethane in tetrahydrofuran;Schlenk technique;Inert atmosphere;Cooling with acetone-dry ice;
References:
Hernández-Toledo, Hugo;Torrens, Hugo;Flores-álamo, Marcos;De Cola, Luisa;Moreno-Alcántar, Guillermo [Chemistry - A European Journal,2021,vol. 27,# 32,p. 8308 - 8314] Location in patent:supporting information
