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2-(ChloroMethyl)-4-phenylnicotinonitrile synthesis

3synthesis methods
3-Pyridinecarbonitrile, 2-(hydroxymethyl)-4-phenyl-

817555-66-1
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2-(ChloroMethyl)-4-phenylnicotinonitrile

817555-70-7
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Yield:817555-70-7 100%

Reaction Conditions:

with methanesulfonyl chloride;triethylamine in dichloromethane at 0 - 20; for 13 h;

References:

Bliznets, Igor V.;Shorshnev, Sergey V.;Aleksandrov, Grigory G.;Stepanov, Aleksandr E.;Lukyanov, Sergey M. [Tetrahedron Letters,2004,vol. 45,# 49,p. 9127 - 9130]