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ChemicalBook CAS DataBase List 2-cyano-5-fluorobenzene-1-sulfonyl chloride
612541-15-8

2-cyano-5-fluorobenzene-1-sulfonyl chloride synthesis

2synthesis methods
-

Yield:612541-15-8 54%

Reaction Conditions:

with phosphorus pentachloride at 120; for 7 h;

References:

Masuda, Naoyuki;Yamamoto, Osamu;Fujii, Masahiro;Ohgami, Tetsuro;Fujiyasu, Jiro;Kontani, Toru;Moritomo, Ayako;Orita, Masaya;Kurihara, Hiroyuki;Koga, Hironobu;Kageyama, Shunji;Ohta, Mitsuaki;Inoue, Hiroshi;Hatta, Toshifumi;Shintani, Masafumi;Suzuki, Hiroshi;Sudo, Kenji;Shimizu, Yasuaki;Kodama, Eiichi;Matsuoka, Masao;Fujiwara, Masatoshi;Yokota, Tomoyuki;Shigeta, Shiro;Baba, Masanori [Bioorganic and Medicinal Chemistry,2005,vol. 13,# 4,p. 949 - 961]