![](/CAS/GIF/15029-38-6.gif)
2-CYANO-N-CYCLOHEXYL-ACETAMIDE synthesis
- Product Name:2-CYANO-N-CYCLOHEXYL-ACETAMIDE
- CAS Number:15029-38-6
- Molecular formula:C9H14N2O
- Molecular Weight:166.22
![Cyclohexylamine](/CAS/20180906/GIF/108-91-8.gif)
108-91-8
585 suppliers
$10.00/5mL
![Ethyl cyanoacetate](/CAS/GIF/105-56-6.gif)
105-56-6
432 suppliers
$10.00/5ml
![2-CYANO-N-CYCLOHEXYL-ACETAMIDE](/CAS/GIF/15029-38-6.gif)
15029-38-6
22 suppliers
$28.60/50MG
Yield:15029-38-6 90%
Reaction Conditions:
with sodium ethanolate in ethanol at 20; for 1 h;
Steps:
4.2. General procedure 1: synthesis of cyanoacetamides 2a-d
General procedure: A mixture of a solution of sodium ethoxide (0.1 mmol) in ethanol (3 mL), ethyl cyanoacetate (10 mmol) and amine (10 mmol) was stirred at room temperature. The reaction time is 1 h for primary amines and 24 h for secondary amine 2d. The precipitate obtained was separated by filtration, washed with diethylether and recrystallised in ethanol to provide a white solid of cyanoacetamides.
References:
Cheikh, Nawel;Bar, Nathalie;Choukchou-Braham, Nourredine;Mostefa-Kara, Bachir;Lohier, Jean-Franois;Sopkova, Jana;Villemin, Didier [Tetrahedron,2011,vol. 67,# 8,p. 1540 - 1551] Location in patent:experimental part
![Cyclohexylamine](/CAS/20180906/GIF/108-91-8.gif)
108-91-8
585 suppliers
$10.00/5mL
![Cyanoacetic acid](/CAS/20180808/GIF/372-09-8.gif)
372-09-8
349 suppliers
$20.00/25g
![2-CYANO-N-CYCLOHEXYL-ACETAMIDE](/CAS/GIF/15029-38-6.gif)
15029-38-6
22 suppliers
$28.60/50MG
![Cyclohexylamine](/CAS/20180906/GIF/108-91-8.gif)
108-91-8
585 suppliers
$10.00/5mL
![1-CYANOACETYL-3,5-DIMETHYLPYRAZOLE](/CAS/GIF/36140-83-7.gif)
36140-83-7
86 suppliers
$23.00/250mg
![2-CYANO-N-CYCLOHEXYL-ACETAMIDE](/CAS/GIF/15029-38-6.gif)
15029-38-6
22 suppliers
$28.60/50MG
![Cyclohexylamine](/CAS/20180906/GIF/108-91-8.gif)
108-91-8
585 suppliers
$10.00/5mL
![2-Cyanoacetamide](/CAS/GIF/107-91-5.gif)
107-91-5
541 suppliers
$5.00/10g
![2-CYANO-N-CYCLOHEXYL-ACETAMIDE](/CAS/GIF/15029-38-6.gif)
15029-38-6
22 suppliers
$28.60/50MG
![Cyclohexylamine](/CAS/20180906/GIF/108-91-8.gif)
108-91-8
585 suppliers
$10.00/5mL
![Methyl cyanoacetate](/CAS/GIF/105-34-0.gif)
105-34-0
428 suppliers
$5.00/25g
![2-CYANO-N-CYCLOHEXYL-ACETAMIDE](/CAS/GIF/15029-38-6.gif)
15029-38-6
22 suppliers
$28.60/50MG