2-CYANOBENZOYL CHLORIDE synthesis
- Product Name:2-CYANOBENZOYL CHLORIDE
- CAS Number:27611-63-8
- Molecular formula:C8H4ClNO
- Molecular Weight:165.58
88-97-1
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 97 percent / Et3N / CH2Cl2 / 8 h / 20 °C
2: 74 percent / aq. NaOH / methanol / 8 h / 20 °C
3: (COCl)2; DMF / CH2Cl2 / 2 h / 20 °C
References:
Shimada, Yoshiaki;Akane, Hiroaki;Taniguchi, Nobuaki;Matsuhisa, Akira;Kawano, Noriyuki;Kikuchi, Kazumi;Yatsu, Takeyuki;Tahara, Atsuo;Tomura, Yuichi;Kusayama, Toshiyuki;Wada, Koh-Ichi;Tsukada, Junko;Tsunoda, Takashi;Tanaka, Akihiro [Chemical and Pharmaceutical Bulletin,2005,vol. 53,# 7,p. 764 - 769]
3839-22-3
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6587-24-2
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136918-14-4
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27611-63-8
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