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ChemicalBook CAS DataBase List 2-(DiMethylcarbaMoyl)benzoic acid, 97%
20320-37-0

2-(DiMethylcarbaMoyl)benzoic acid, 97% synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: thionyl chloride / dichloromethane / 6 h / 50 °C / Inert atmosphere
2: water / 0 °C / Inert atmosphere
3: dichloromethane / 1.5 h / 20 °C / Inert atmosphere
4: chloroform / 72 h / 68 °C / 1050.11 Torr

References:

Frutos-Pedreno, Roberto;Gonzalez-Herrero, Pablo;Vicente, Jose;Jones, Peter G. [Organometallics,2013,vol. 32,# 16,p. 4664 - 4676]

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