ChemicalBook CAS DataBase List 2-(diphenylamino)phenylboronic acid

2-(diphenylamino)phenylboronic acid synthesis

5synthesis methods

Product Name:2-(diphenylamino)phenylboronic acid
CAS Number:934169-37-6
Molecular formula:C18H16BNO2
Molecular Weight:289.14

150-46-9
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78600-31-4 Synthesis

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Yield:934169-37-6 82%

Reaction Conditions:

Stage #1: (2-bromophenyl)diphenylaminewith n-butyllithium in tetrahydrofuran;hexane at -78; for 1 h;
Stage #2: triethyl borate in tetrahydrofuran;hexane at -78 - 20; for 18 h;

References:

De los Santos, Zeus A.;Lynch, Ciarán C.;Wolf, Christian [Chemistry - A European Journal,2022,vol. 28,# 61,art. no. E202202028] Location in patent:supporting information