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ChemicalBook CAS DataBase List 2-Dodecene

2-Dodecene synthesis

10synthesis methods
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Yield:112-41-4 96% ,1652-96-6 2%

Reaction Conditions:

with [(dimethylphenylsilyl)methyl]magnesium chloride;1,3-bis(mesityl)imidazolium chloride;cobalt(II) chloride in tetrahydrofuran;1,4-dioxane at 25; for 0.5 h;Inert atmosphere;regioselective reaction;

References:

Kobayashi, Tsuneyuki;Ohmiya, Hirohisa;Yorimitsu, Hideki;Oshima, Koichiro [Journal of the American Chemical Society,2008,vol. 130,# 34,p. 11276 - 11277] Location in patent:supporting information; experimental part