2-Fluoro-4-iodo-3-(2-methylallyl)pyridine synthesis
- Product Name:2-Fluoro-4-iodo-3-(2-methylallyl)pyridine
- CAS Number:744257-62-3
- Molecular formula:C9H9FIN
- Molecular Weight:277.08
1458-98-6
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113975-22-7
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744257-62-3
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Yield:744257-62-3 93%
Reaction Conditions:
Stage #1: 2-fluoro-3-iodopyridinewith n-butyllithium;diisopropylamine in tetrahydrofuran;hexane at -78; for 1 h;
Stage #2: 2-methyl-3-bromo-1-propene in tetrahydrofuran;hexane at -78 - -45; for 4.5 h;Further stages.;
References:
Saitton, Stina;Kihlberg, Jan;Luthman, Kristina [Tetrahedron,2004,vol. 60,# 29,p. 6113 - 6120]
372-48-5
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744257-62-3
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