2-Fluoro-6-methoxy-4-methylbenzaldehyde synthesis
- Product Name:2-Fluoro-6-methoxy-4-methylbenzaldehyde
- CAS Number:1362295-77-9
- Molecular formula:C9H9FO2
- Molecular Weight:168.16
216976-31-7
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: caesium carbonate / N,N-dimethyl-formamide / 0.67 h / 20 °C
2.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran; hexane; cyclohexane / 2 h / -78 °C
2.2: 1 h / -78 °C
References:
Sather, Aaron C.;Berryman, Orion B.;Rebek, Julius [Organic Letters,2012,vol. 14,# 6,p. 1600 - 1603]