(2-formylphenoxy)acetonitrile(SALTDATA: FREE) synthesis
3synthesis methods
- Product Name:(2-formylphenoxy)acetonitrile(SALTDATA: FREE)
- CAS Number:125418-83-9
- Molecular formula:C9H7NO2
- Molecular Weight:161.16
Yield:125418-83-9 99%
Reaction Conditions:
Stage #1: salicylaldehydewith potassium carbonate in N,N-dimethyl-formamide at 20; for 0.25 h;Schlenk technique;Inert atmosphere;
Stage #2: bromoacetonitrile in N,N-dimethyl-formamide at 20; for 4 h;
References:
Wang, Ali;Xie, Xin;Zhang, Chunli;Liu, Yuanhong [Chemical Communications,2020,vol. 56,# 99,p. 15581 - 15584] Location in patent:supporting information