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2-Hexylthieno[3,4-b]thiophene synthesis

6synthesis methods
Thieno[3,4-b]thiophene, 2-hexyl-4,6-dihydro-

1202695-59-7
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2-Hexylthieno[3,4-b]thiophene

1202695-55-3
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Yield:1202695-55-3 54%

Reaction Conditions:

with 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane at 0; for 0.5 h;

References:

Dey, Tanmoy;Navarathne, Daminda;Invernale, Michael A.;Berghorn, Ian D.;Sotzing, Gregory A. [Tetrahedron Letters,2010,vol. 51,# 16,p. 2089 - 2091] Location in patent:supporting information; experimental part