2-hydroxy-6-(methoxymethoxy)benzaldehyde synthesis
- Product Name:2-hydroxy-6-(methoxymethoxy)benzaldehyde
- CAS Number:84290-49-3
- Molecular formula:C9H10O4
- Molecular Weight:182.17
57234-29-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane / 2 h / -10 °C / Inert atmosphere
1.2: 1 h / 0 °C / Inert atmosphere
2.1: hydrogenchloride / water; tetrahydrofuran / 1.5 h / Inert atmosphere
References:
GLOBAL BLOOD THERAPEUTICS, INC.;LI, Zhe WO2015/31285, 2015, A1
79834-12-1
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1000210-73-0
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