2-(HydroxyMethyl)hoMoMorpholine synthesis
- Product Name:2-(HydroxyMethyl)hoMoMorpholine
- CAS Number:1207254-23-6
- Molecular formula:C6H13NO2
- Molecular Weight:131.17
1031442-66-6
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1207254-23-6
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Yield:-
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in ethanol for 4 h;
Steps:
106.3
To a solution of 4-Benzyl-[1,4]oxazepan-2-yl)-methanol (1 gm, 0.004 mol) in ethanol 10% Pd-C was added. The reaction mixture was then subjected to hydrogenation for 4 hours. Then it was filtered and concentrated to produce (550 mg, 93.2%) [1,4]Oxazepan-2-yl-methanol. LC/MS [M+H]+: 132.0.
References:
KHAMRAI, Uttam;Karak, Sumit Kumar;Ronsheim, Matthew;Saha, Ashis Kumar US2010/168080, 2010, A1 Location in patent:Page/Page column 89
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1207254-23-6
25 suppliers
$45.00/10mg