2-HydroxyMethylpyrrolidine synthesis
- Product Name:2-HydroxyMethylpyrrolidine
- CAS Number:10200-26-7
- Molecular formula:C5H11NO
- Molecular Weight:101.1469
609-36-9
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Yield:10200-26-7 96%
Reaction Conditions:
Stage #1: rac-Pro-OHwith lithium aluminium tetrahydride in tetrahydrofuran at 0;Inert atmosphere;Reflux;
Stage #2: with water;potassium hydroxide in tetrahydrofuran at 20;
References:
Tang, Yi-Qiang;Lu, Jian-Mei;Wang, Xiu-Ren;Shao, Li-Xiong [Tetrahedron,2010,vol. 66,# 40,p. 7970 - 7974] Location in patent:experimental part
149-87-1
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41222-21-3
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617-65-2
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2812-47-7
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