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ChemicalBook CAS DataBase List 2-IODO-3-BROMOFLUOROBENZENE

2-IODO-3-BROMOFLUOROBENZENE synthesis

2synthesis methods
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Yield:450412-29-0 93%

Reaction Conditions:

Stage #1:3-fluorobromobenzene with tBu2Zn(TMP)Li in tetrahydrofuran at -30; for 24 h;
Stage #2: with iodine in tetrahydrofuran at 20;Further stages.;

References:

Uchiyama, Masanobu;Miyoshi, Tomoko;Kajihara, Yumiko;Sakamoto, Takao;Otani, Yuko;Ohwada, Tomohiko;Kondo, Yoshinori [Journal of the American Chemical Society,2002,vol. 124,# 29,p. 8514 - 8515]

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