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2-(IODOMETHYL)-1,1,1,3,3,3-HEXAFLUOROPROPANE synthesis

1synthesis methods
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Yield:883499-40-9 68%

Reaction Conditions:

with hydrogen iodide in dichloromethane;water at 20; for 3 h;

References:

Arduengo III, Anthony J.;Dolphin, Joshua S.;Gurau, Gabriela;Marshall, William J.;Nelson, Joseph C.;Petrov, Viacheslav A.;Runyon, Jason W. [Angewandte Chemie - International Edition,2013,vol. 52,# 19,p. 5110 - 5114][Angew. Chem.,2013,vol. 125,# 19,p. 5214 - 5218] Location in patent:supporting information