(2-Methoxy-3-methylphenyl)methanol synthesis
- Product Name:(2-Methoxy-3-methylphenyl)methanol
- CAS Number:74090-48-5
- Molecular formula:C9H12O2
- Molecular Weight:152.19
52239-62-0
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Yield:-
Reaction Conditions:
with lithium borohydride in methanol;diethyl ether at 0; for 0.583333 h;
Steps:
19
LiBH4 (5.10 g, 0.23 mmol) was added to a solution of 2-methoxy-3-methyl-benzoic acid methyl ester (8.46 g, 47.00 mmol) in Et2O at 0° C. The reaction mixture was stirred for 5 minutes, MeOH (9.50 mL, 0.23 mmol) was added in a dropwise fashion. The reaction mixture was then stirred for 30 minutes, and was quenched into 1N NaOH. The resulting solution was extracted with Et2O (3×200 mL) and the combined organic phases were washed with brine (1×150 mL), dried over MgSO4 and concentrated to afford the title compound.
References:
US2008/194650,2008,A1 Location in patent:Page/Page column 23-24
83-40-9
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23287-26-5
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