![](/CAS/GIF/97-52-9.gif)
2-Methoxy-4-nitroaniline synthesis
- Product Name:2-Methoxy-4-nitroaniline
- CAS Number:97-52-9
- Molecular formula:C7H8N2O3
- Molecular Weight:168.15
![N-(2-METHOXY-4-NITROPHENYL)ACETAMIDE](/CAS/GIF/93-27-6.gif)
93-27-6
32 suppliers
inquiry
![2-Methoxy-4-nitroaniline](/CAS/GIF/97-52-9.gif)
97-52-9
241 suppliers
$10.00/5g
Yield:97-52-9 95.3%
Reaction Conditions:
with water;sodium hydroxide at 100; for 2 h;Temperature;
Steps:
1.3; 21-28; 29; 30; 2.3; 3.3
General procedure: 3), the 2-methoxy-4-nitroacetanilide obtained in the step 2) is added to 200 g of water, and 48.0 g (1.2 mol) of sodium hydroxide is added.After heating to 100 ° C, the hydrolysis reaction was kept for 2 h.GC detection of 2-methoxy-4-nitroacetanilide has been completed,The reaction solution was cooled to 0 to 5 ° C and filtered.The obtained filter cake is washed (300 ml of deionized water),Drying (drying to constant weight at 80 ° C) gives the product 2-methoxy-4-nitroaniline 159.4g,The yield was 94.8%,
References:
CN109776337,2019,A Location in patent:Paragraph 0051; 0054; 0064; 0065; 0067-0073; 0078
![2'-METHOXY-4'-NITROFORMANILIDE](/CAS/20180703/GIF/71862-04-9.gif)
71862-04-9
2 suppliers
$28.60/250mg
![2-Methoxy-4-nitroaniline](/CAS/GIF/97-52-9.gif)
97-52-9
241 suppliers
$10.00/5g
![1-Triazene, 3-(2-methoxy-4-nitrophenyl)-1-(4-methylphenyl)-](/CAS/20210305/GIF/869373-61-5.gif)
869373-61-5
0 suppliers
inquiry
![4-Methoxyphenylboronic acid](/CAS/GIF/5720-07-0.gif)
5720-07-0
454 suppliers
$6.00/5g
![4-METHOXY-4'-METHYLBIPHENYL](/CAS/GIF/53040-92-9.gif)
53040-92-9
34 suppliers
$365.00/1g
![2-Methoxy-4-nitroaniline](/CAS/GIF/97-52-9.gif)
97-52-9
241 suppliers
$10.00/5g
![1,4-diamino-2-methoxybenzene](/CAS/GIF/5307-02-8.gif)
5307-02-8
19 suppliers
inquiry
![2-Methoxy-4-nitroaniline](/CAS/GIF/97-52-9.gif)
97-52-9
241 suppliers
$10.00/5g
![2-CHLORO-5-NITROANISOLE](/CAS/GIF/1009-36-5.gif)
1009-36-5
177 suppliers
$12.00/1g
![2-Methoxy-4-nitroaniline](/CAS/GIF/97-52-9.gif)
97-52-9
241 suppliers
$10.00/5g