2-Methoxyphenylacetonitrile synthesis
- Product Name:2-Methoxyphenylacetonitrile
- CAS Number:7035-03-2
- Molecular formula:C9H9NO
- Molecular Weight:147.17
578-57-4
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$6.00/10g
105-56-6
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$10.00/5ml
7035-03-2
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$14.14/1gm:
Yield:7035-03-2 82%
Reaction Conditions:
Stage #1:2-bromoanisole;ethyl 2-cyanoacetate with potassium phosphate;N-(2-methylnaphthalen-1-yl)-N’-(pyridin-2-ylmethyl)oxalamide;copper(l) chloride in ethanol at 80; for 24 h;Schlenk technique;Inert atmosphere;
Stage #2: with water in ethanol at 80;Schlenk technique;Inert atmosphere;Cooling;
References:
Chen, Ying;Xu, Lanting;Jiang, Yongwen;Ma, Dawei [Angewandte Chemie - International Edition,2021,vol. 60,# 13,p. 7082 - 7086][Angew. Chem.,2021,vol. 133,# 13,p. 7158 - 7162,5] Location in patent:supporting information
33390-80-6
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7035-03-2
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7035-02-1
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$59.00/10 g
75-86-5
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7035-03-2
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766-51-8
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1071-36-9
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7035-03-2
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