![](/CAS/GIF/768-49-0.gif)
2-METHYL-1-PHENYLPROPENE synthesis
- Product Name:2-METHYL-1-PHENYLPROPENE
- CAS Number:768-49-0
- Molecular formula:C10H12
- Molecular Weight:132.2
![2-Methyl-1-phenyl-2-propanol](/CAS/GIF/100-86-7.gif)
100-86-7
300 suppliers
$8.00/25g
![2-METHYL-1-PHENYLPROPENE](/CAS/GIF/768-49-0.gif)
768-49-0
109 suppliers
$18.00/100mg
Yield:768-49-0 80%
Reaction Conditions:
with aluminum (III) chloride;triphenylphosphine in nitromethane at 80; for 2 h;
Steps:
2.2. A typical alcohol dehydration procedure
General procedure: In a typical reaction, alcohol (0.4 mmol) was mixed with AlCl3 (0.02 mmol, 5 mol%) and triphenylphosphine (PPh3, 0.02 mmol, 5 mol%) in nitromethane (1.0 mL). Thereafter the mixture was stirred at 80 °C for 2 h. After the reaction, the mixture was cooled to room temperature, and the product was isolated using preparative thin layer chromatography (TLC, eluting solution: petroleum ether/ethyl acetate, 5/1 (v/v)). Tests for substrate scope were all performed with an analogous procedure.
References:
Liu, Changhui;Pan, Bin;Gu, Yanlong [Cuihua Xuebao/Chinese Journal of Catalysis,2016,vol. 37,# 6,p. 979 - 986]
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$29.00/5mL
![2-METHYL-1-PHENYLPROPENE](/CAS/GIF/768-49-0.gif)
768-49-0
109 suppliers
$18.00/100mg
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inquiry
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$45.00/50mg
![2-METHYL-1-PHENYLPROPENE](/CAS/GIF/768-49-0.gif)
768-49-0
109 suppliers
$18.00/100mg
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24470-78-8
181 suppliers
$5.00/5g
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100-52-7
943 suppliers
$17.30/2g
![2-METHYL-1-PHENYLPROPENE](/CAS/GIF/768-49-0.gif)
768-49-0
109 suppliers
$18.00/100mg