2-METHYL-1-PHENYLPROPENE synthesis
- Product Name:2-METHYL-1-PHENYLPROPENE
- CAS Number:768-49-0
- Molecular formula:C10H12
- Molecular Weight:132.2
100-86-7
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$8.00/25g
768-49-0
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$18.00/100mg
Yield:768-49-0 80%
Reaction Conditions:
with aluminum (III) chloride;triphenylphosphine in nitromethane at 80; for 2 h;
Steps:
2.2. A typical alcohol dehydration procedure
General procedure: In a typical reaction, alcohol (0.4 mmol) was mixed with AlCl3 (0.02 mmol, 5 mol%) and triphenylphosphine (PPh3, 0.02 mmol, 5 mol%) in nitromethane (1.0 mL). Thereafter the mixture was stirred at 80 °C for 2 h. After the reaction, the mixture was cooled to room temperature, and the product was isolated using preparative thin layer chromatography (TLC, eluting solution: petroleum ether/ethyl acetate, 5/1 (v/v)). Tests for substrate scope were all performed with an analogous procedure.
References:
Liu, Changhui;Pan, Bin;Gu, Yanlong [Cuihua Xuebao/Chinese Journal of Catalysis,2016,vol. 37,# 6,p. 979 - 986]
100-52-7
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67-64-1
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563-79-1
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$29.00/5mL
768-49-0
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$18.00/100mg
588-59-0
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611-69-8
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768-49-0
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$18.00/100mg
24470-78-8
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$5.00/5g
100-52-7
968 suppliers
$17.30/2g
768-49-0
118 suppliers
$18.00/100mg