2-METHYL-3-[4-METHYL(3,5-OXAZOLYL)]PROP-2-ENAL synthesis

6synthesis methods

Product Name:2-METHYL-3-[4-METHYL(3,5-OXAZOLYL)]PROP-2-ENAL
CAS Number:139630-91-4
Molecular formula:C8H9NO2
Molecular Weight:151.16

2-METHYL-OXAZOLE-4-CARBOXYLIC ACID METHYL ESTER

85806-67-3
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$11.00/250mg

2-METHYL-3-[4-METHYL(3,5-OXAZOLYL)]PROP-2-ENAL

139630-91-4
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 65 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 3 h / -78 °C
2: 94 percent / oxalyl chloride; dimethylsulfoxide; triethylamine / CH₂Cl₂ / -60 - 20 °C
3: 91 percent / benzene / 72 h / 20 °C

References:

Lafontaine, Jennifer A.;Provencal, David P.;Gardelli, Cristina;Leahy, James W. [Journal of Organic Chemistry,2003,vol. 68,# 11,p. 4215 - 4234]

2-(TRIPHENYLPHOSPHORANYLIDENE)PROPIONALDEHYDE

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$57.20/1g

113732-84-6
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139630-91-4
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References

141567-53-5
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$90.00/100mg

139630-91-4
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References

4-Oxazolecarboxylicacid,4,5-dihydro-2-methyl-,methylester,(4S)-(9CI)

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139630-91-4
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References

10200-43-8 Synthesis

10200-43-8
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$16.00/100mg

139630-91-4
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References