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2'-METHYL-3-(4-METHYLPHENYL)PROPIOPHENONE synthesis

2synthesis methods
39627-62-8 Synthesis
1-o-tolylprop-2-en-1-ol

39627-62-8
2 suppliers
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1576-35-8 Synthesis
4-Methylbenzenesulfonhydrazide

1576-35-8
449 suppliers
$10.00/1g

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Yield:898768-42-8 74%

Reaction Conditions:

with tetrabutylammomium bromide;oxygen;palladium diacetate in water;dimethyl sulfoxide;N,N-dimethyl-formamide at 120; under 760.051 Torr;Schlenk technique;Heck Reaction;

References:

Huang, Liangbin;Qi, Ji;Wu, Xia;Wu, Wanqing;Jiang, Huanfeng [Chemistry - A European Journal,2013,vol. 19,# 46,p. 15462 - 15466] Location in patent:supporting information