2-METHYL-4-CYANOPHENYLBORONIC ACID synthesis
- Product Name:2-METHYL-4-CYANOPHENYLBORONIC ACID
- CAS Number:313546-18-8
- Molecular formula:C8H8BNO2
- Molecular Weight:160.97
41963-20-6
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313546-18-8
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / -98 °C
1.2: tetrahydrofuran; hexane / 3.5 h / -98 - 20 °C
2.1: 0.63 g / aq. HCl / diethyl ether
References:
Stones, Duane;Manku, Sukhdev;Lu, Xiaosong;Hall, Dennis G. [Chemistry - A European Journal,2004,vol. 10,# 1,p. 92 - 100]