![](/CAS/GIF/14314-21-7.gif)
2-methyl-6-methyleneoct-7-en-4-ol synthesis
- Product Name:2-methyl-6-methyleneoct-7-en-4-ol
- CAS Number:14314-21-7
- Molecular formula:C10H18O
- Molecular Weight:154.25
![Isovaleraldehyde](/CAS/GIF/590-86-3.gif)
590-86-3
353 suppliers
$10.00/5g
![2-methyl-6-methyleneoct-7-en-4-ol](/CAS/GIF/14314-21-7.gif)
14314-21-7
16 suppliers
inquiry
Yield: 65%
Steps:
6 2-Methyl-6-methylene-7-octen-4-ol (ipsenol)
EXAMPLE 6 2-Methyl-6-methylene-7-octen-4-ol (ipsenol) Following the method of Example 2, the title compound was prepared at 0° C. from isovaleraldehyde in 65% yield. bp 92°-94° C./19 mm Hg. 1 H NMR: (CDCl3), δ0.88 (3H, d, J=6 Hz), 0.92 (3H, d, J=6 Hz), 1.2 (2H, m), 1.8 (2H, m), 3.72 (1H, m), 5.0-5.3 (4H, m), 6.3 (1H, dd, J=12 Hz). 13 C NMR: (CDCl3), δ: 22.26, 23.63, 24.87, 40.79, 46.69, 67.88, 114.59, 118.86, 139.05, 143.7.
References:
Aldrich Chemical Company, Inc. US5103063, 1992, A
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
0 suppliers
inquiry
![2-methyl-6-methyleneoct-7-en-4-ol](/CAS/GIF/14314-21-7.gif)
14314-21-7
16 suppliers
inquiry
![Isovaleraldehyde](/CAS/GIF/590-86-3.gif)
590-86-3
353 suppliers
$10.00/5g
![Isoprene](/CAS/GIF/78-79-5.gif)
78-79-5
250 suppliers
$14.56/25ML
![3,6-dihydro-4-methyl-2-(2-methylpropyl)-2H-pyran](/CAS/GIF/59848-69-0.gif)
59848-69-0
1 suppliers
inquiry
![2-methyl-6-methyleneoct-7-en-4-ol](/CAS/GIF/14314-21-7.gif)
14314-21-7
16 suppliers
inquiry